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EnglishA gas liquid chromatograph (GLC) equipped with a nitrogen-phosphorus detector (NPD) was used for the analysis of 8 organophosphorus pesticides in milk: acephate, chlorpyriphos, chlorpyriphos-methyl, diazinon, methamidophos, methidation, phorate, pirimiphos-methyl. The isolation of these pesticides was performed by liquid partition followed by a cleanup with a solid phase cartridge. The limit of quantification (LOQ) and limit of detection (LOD) were respectively 5 ppb and 1 ppb for each compound. The method was finally tested on milk samples.
| Titolo: | Proposal of an analytical method for determination of residues of organophosphorus pesticides in milk by GLC-NPD |
| Autore/i: | PAGLIUCA, GIAMPIERO; GAZZOTTI, TERESA; ZIRONI, ELISA; PAVONCELLI N.; ROSMINI, ROBERTO |
| Autore/i Unibo: | |
| Anno: | 2004 |
| Rivista: | |
| Pagina iniziale: | 257 |
| Pagina finale: | 259 |
| Digital Object Identifier (DOI): | http://dx.doi.org/10.1023/B:VERC.0000045420.62584.2c |
| Abstract: | A gas liquid chromatograph (GLC) equipped with a nitrogen-phosphorus detector (NPD) was used for the analysis of 8 organophosphorus pesticides in milk: acephate, chlorpyriphos, chlorpyriphos-methyl, diazinon, methamidophos, methidation, phorate, pirimiphos-methyl. The isolation of these pesticides was performed by liquid partition followed by a cleanup with a solid phase cartridge. The limit of quantification (LOQ) and limit of detection (LOD) were respectively 5 ppb and 1 ppb for each compound. The method was finally tested on milk samples. |
| Data prodotto definitivo in UGOV: | 30-set-2005 |
| Appare nelle tipologie: | 4.01 Contributo in Atti di convegno |
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