The aim of the present work was to develop a sensitive and selective method for identification and quantification of fumonisin B1 (FB1) in milk. FB1 was isolated from milk, by a single step immunoaffinity column and was detected using liquid chromatography coupled with tandem mass spectrometry in positive electrospray ionization (ESI+). The analysis were carried out in multiple reaction monitoring (MRM) mode using the two main product ions. The good performances of the proposed method can assure a correct fumonisin detection in milk even at relatively low concentrations.

Determinazione di fumonisina B1 in latte mediante LC-MS/MS

GAZZOTTI, TERESA;LUGOBONI, BARBARA;ZIRONI, ELISA;BARBAROSSA, ANDREA;GIACOMETTI, FEDERICA;SERRAINO, ANDREA;PAGLIUCA, GIAMPIERO
2008

Abstract

The aim of the present work was to develop a sensitive and selective method for identification and quantification of fumonisin B1 (FB1) in milk. FB1 was isolated from milk, by a single step immunoaffinity column and was detected using liquid chromatography coupled with tandem mass spectrometry in positive electrospray ionization (ESI+). The analysis were carried out in multiple reaction monitoring (MRM) mode using the two main product ions. The good performances of the proposed method can assure a correct fumonisin detection in milk even at relatively low concentrations.
Sicurezza alimentare: l'approccio del veterinario igienista ad una problematica in continua evoluzione
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Gazzotti T.; Lugoboni B.; Zironi E.; Barbarossa A.; Giacometti F.; Serraino A.; Pagliuca G.
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Utilizza questo identificativo per citare o creare un link a questo documento: http://hdl.handle.net/11585/62741
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