The aim of the present work was to develop a sensitive and selective method for identification and quantification of fumonisin B1 (FB1) in milk. FB1 was isolated from milk, by a single step immunoaffinity column and was detected using liquid chromatography coupled with tandem mass spectrometry in positive electrospray ionization (ESI+). The analysis were carried out in multiple reaction monitoring (MRM) mode using the two main product ions. The good performances of the proposed method can assure a correct fumonisin detection in milk even at relatively low concentrations.
Gazzotti T., Lugoboni B., Zironi E., Barbarossa A., Giacometti F., Serraino A., et al. (2008). Determinazione di fumonisina B1 in latte mediante LC-MS/MS. s.l : Associazione Italiana Veterinari Igienisti.
Determinazione di fumonisina B1 in latte mediante LC-MS/MS
GAZZOTTI, TERESA;LUGOBONI, BARBARA;ZIRONI, ELISA;BARBAROSSA, ANDREA;GIACOMETTI, FEDERICA;SERRAINO, ANDREA;PAGLIUCA, GIAMPIERO
2008
Abstract
The aim of the present work was to develop a sensitive and selective method for identification and quantification of fumonisin B1 (FB1) in milk. FB1 was isolated from milk, by a single step immunoaffinity column and was detected using liquid chromatography coupled with tandem mass spectrometry in positive electrospray ionization (ESI+). The analysis were carried out in multiple reaction monitoring (MRM) mode using the two main product ions. The good performances of the proposed method can assure a correct fumonisin detection in milk even at relatively low concentrations.I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.
