In this paper, a Q-tube equipment is proposed as a valid alternative to monomode MW technology to synthesize in a simple and economic way a library of dihydropyrimidine derivatives performing the Biginelli reaction in solvent-free conditions under pressure and with the catalysis of a very mild and environmentally benign Lewis acid consisting of erbium trichloride hexahydrate. © 2014 American Chemical Society.
Facile ecofriendly synthesis of monastrol and its structural isomers via biginelli reaction / Oliverio, Manuela; Costanzo, Paola; Nardi, Monica; Rivalta, Ivan; Procopio, Antonio*. - In: ACS SUSTAINABLE CHEMISTRY & ENGINEERING. - ISSN 2168-0485. - STAMPA. - 2:5(2014), pp. 1228-1233. [10.1021/sc5000682]
Facile ecofriendly synthesis of monastrol and its structural isomers via biginelli reaction
Rivalta, Ivan;
2014
Abstract
In this paper, a Q-tube equipment is proposed as a valid alternative to monomode MW technology to synthesize in a simple and economic way a library of dihydropyrimidine derivatives performing the Biginelli reaction in solvent-free conditions under pressure and with the catalysis of a very mild and environmentally benign Lewis acid consisting of erbium trichloride hexahydrate. © 2014 American Chemical Society.I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.