2,9-Dimethyl-11-(3-pentadecylphenoxy)dibenzo[c,f][1,2,5]dithiaphosphepine 11-oxide was synthesized (yield 50%) by a two-step procedure. The first step starts with a benzothiadiphosphole and bis-Grignard reagent, and the second step consists of adding the sodium salt of a derivative of cardanol. The structure of newly synthesized compound was elucidated based on1H-NMR,13C-NMR,31P-NMR, IR, Electron Spray Ionization (ESI)–MS, Gas Chromatography- Mass Spectroscopy (GC–MS), and Electron Spray Ionization-High Resolution Mass Spectroscopy (ESI–HRMS).
2,9-dimethyl-11-(3- pentadecylphenoxy)dibenzo[c,f][1,2,5]dithiaphosphe pine 11-oxide / Micheletti G.; Mazzacurati M.; Telese D.; Boga C.. - In: MOLBANK. - ISSN 1422-8599. - ELETTRONICO. - 2020:1(2020), pp. M1109.1-M1109.4. [10.3390/M1109]
2,9-dimethyl-11-(3- pentadecylphenoxy)dibenzo[c,f][1,2,5]dithiaphosphe pine 11-oxide
Micheletti G.
Membro del Collaboration Group
;Mazzacurati M.Membro del Collaboration Group
;Telese D.Membro del Collaboration Group
;Boga C.
Membro del Collaboration Group
2020
Abstract
2,9-Dimethyl-11-(3-pentadecylphenoxy)dibenzo[c,f][1,2,5]dithiaphosphepine 11-oxide was synthesized (yield 50%) by a two-step procedure. The first step starts with a benzothiadiphosphole and bis-Grignard reagent, and the second step consists of adding the sodium salt of a derivative of cardanol. The structure of newly synthesized compound was elucidated based on1H-NMR,13C-NMR,31P-NMR, IR, Electron Spray Ionization (ESI)–MS, Gas Chromatography- Mass Spectroscopy (GC–MS), and Electron Spray Ionization-High Resolution Mass Spectroscopy (ESI–HRMS).| File | Dimensione | Formato | |
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